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1.
Vijay Singh Sharanagat Prabhat K. Nema Lochan Singh Ankur Kumar 《International Journal of Food Science & Technology》2022,57(3):1654-1665
The effect of microwave roasting parameters (300, 450 and 600 W; 5, 10 and 15 min) on acrylamide content in sorghum grain was determined using High Pressure Liquid Chromatography (HPLC)-photo diode array (PDA) detector coupled with C-18 column. Samples roasted at 300 and 450 W did not possess acrylamide, whereas 600 W (15 min) favoured formation of 2740.19 µg/kg of acrylamide, levels far exceeding the defined European Union (EU) limits. The chronic daily intake (CDI) for acrylamide through consumption of such grain flour was 3.25–9.5-fold higher to Joint FAO/WHO Expert Committee on Food Additives (JECFA) defined high exposure limits. The margin of exposure (MOE) values ranged from 4.3 to 12.76 and from 11.07 to 32.27 for neoplastic and neurological effects, respectively, demonstrating high exposure and serious health concerns associated with dietary intake of this toxicant. This study assesses the risk for the Indian population and highlights the importance of optimising process parameters for food product to minimise such exposure risks. 相似文献
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The effect of biochar substituted for anthracite as reductant on magnetizing-roasting pyrite cinder was investigated.The key of magnetizing-roasting is the gasification reaction between reductants and CO2.Since biochar could react with CO2 more rapidly at lower temperature,the reactivity of biochar is better than that of anthracite.The gasification of biochar could produce reducing condition ofφCO/(φCO+φCO2)about 10%-20% between 700-800 ℃,which is in accord with the atmosphere and temperature of Fe2O3 reduction.So it is beneficial to the reduction of iron mineral of pyrite cinder.Compared with anthracite,biochar could decrease the roasting temperature from825 to 750 ℃ and roasting time from 20 to 15min,which shows that a better effect of magnetization could be obtained in the condition of lower temperature and shorter time.Using biochar as reductant,iron concentrate extracted from pyrite cinder as about 64%iron grade could be produced,and the recovery is over 90% under the condition of above 90% grinding particle less than 0.045 mm and magnetic intensity of 0.124-0.194 T. 相似文献
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对钙化?酸浸提钒沉钒母液中锰资源的回收,一方面可以提升提钒工艺的经济效益,另一方面可避免母液循环时锰浓度不断累积而影响氧化钒产品质量,从而有助于实现母液闭路循环而提升全流程的环境效益。本工作提出了采用草酸沉淀法高效回收沉钒母液中的Mn2+,考察溶液体系pH值、草酸加量系数、反应温度和时间对锰回收率及沉淀产物物相组成的影响,以及草酸沉淀分离锰后母液的循环次数对钒浸出过程的影响。结果表明,草酸沉淀法可高效分离沉钒母液中的Mn2+,在溶液体系pH=4.0、草酸加量系数为1.5、反应温度为50℃、反应时间为60 min的条件下,锰回收率达94.33%,所得产物为纯度大于98%的水合草酸锰,为片状晶体,并呈花簇状生长。将脱锰后的沉钒母液循环至酸浸段,对钒浸出率及浸出液中锰的浓度没有明显影响,表明该方法有助于实现钙化?酸浸提钒中废水的闭路循环。 相似文献
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主要针对我国多金属硫化物勘探合同区样品产出的精矿开展冶炼工艺方案研究,考察其冶金性能,综合回收其有价金属。通过试验研究,富锌多金属硫化物精矿经焙烧-酸浸后,锌和铜浸出率可分别达到99.22%和96.71%,贵金属主要富集于浸出渣中,为我国大洋多金属硫化物的冶金技术开发提供依据。 相似文献
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《中国稀土学报(英文版)》2022,40(6):981-987
Based on the new process named “Combination Method” for metallurgy and separation of Baotou mixed rare earth concentrate (BMREC), the aim of this paper is to clearly elucidate the phase change behavior of BMREC without additives during oxidative roasting at 450–800 °C. The results indicate that the bastnaesite in BMREC is decomposed at 450–550 °C, the weight loss is about 10.3 wt%, and the activation energy (E) is 144 kJ/mol. The bastnaesite in BMREC is decomposed into rare earth fluoride, rare earth oxides (La2O3, Ce7O12, Pr6O11 and Nd2O3), and CO2, particularly, with the increase of roasting temperature, bastnaesite in BMREC is more completely decomposed into LaF3, which causes a decrease in leaching rate of La during the HCl leaching process. Additionally, the maximum cerium oxidation efficiency reaches about 60 wt% when the roasting temperature is equal to or above 500 °C, and the oxidation reaction rate of cerium increases with the increasing roasting temperature. 相似文献
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Fiseha Tesfaye Dmitry Sukhomlinov Daniel Lindberg Mykola Moroz Pekka Taskinen Leena Hupa 《Mineral Processing and Extractive Metallurgy Review》2019,40(1):67-78
In this article, oxidation processes of Ag-Bi-Sb-based phases were investigated. Synthesized AgBiS2 and AgSbS2-Sb2S3-Sb samples were thermally analyzed in synthetic air by applying the simultaneous DSC-TGA analysis technique. The oxidation processes at PO?=0.2 atm and T<1173 K were observed to take place in many-step sequence of various reactions with an overall reaction 2AgMeS2 + 5.5O2(g) ? 2Ag + Me2O3 + 4SO2(g), where Me=(Bi,Sb). Oxidations of AgBiS2, Sb2S3, and AgSbS2 were observed to begin above 549±2K, 610±2K, and 733±2K, respectively. Furthermore, oxidation processes of AgBi3S5 and Ag3SbS3 were estimated, and thermodynamic functions for the overall oxidation reactions were calculated and discussed. 相似文献
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《中国有色金属学会会刊》2020,30(4):1111-1123
A novel process based on chlorination roasting was proposed to simultaneously recover gold and zinc from refractory carbonaceous gold ore by using NaCl as chlorination agent. The effects of roasting temperature, roasting time and NaCl content on the volatilization rates of gold and zinc were investigated. The reaction mechanism and the phase transition process were also analyzed by means of SEM, EDS and XRD. The results demonstrated that under the optimal conditions of NaCl content of 10%, roasting temperature of 800 °C, roasting time of 4 h and gas flow rate of 1 L/min, the rates of gold and zinc were 92% and 92.56%, respectively. During low-temperature chlorination roasting stage, a certain content of sulfur was beneficial to the chlorination reactions of gold and zinc; and during high-temperature chlorination roasting stage, the crystal structure of vanadium-bearing mica was destroyed, and the vanadium-containing oxides were beneficial to the chlorinating volatilization of gold and zinc. Eventually, the chlorinated volatiles of gold and zinc could be recovered by alkaline solution. 相似文献